Items | ATD Conditions | |
---|---|---|
Split ratio | 10 : 1 | |
Carrier GAS | He (99.999%) | |
TDS flow | 1 mL/min | |
Desorption temperature program | Initial temperature | 30°C (holding 3 min) |
Final temperature | 60°C/min, 280°C, (holding 5 min) | |
CIS temperature program | Initial temperature | −30°C (holding 5 min) |
Final temperature | 12°C/min, 280°C, (holding 5 min) | |
Transfer line temperature | 300°C |