Table 2. 13C-NMR Spectral data of compounds (a-d; figure 3) isolated from dichloromethane (CH2Cl2) fraction sclerotium of W. hoelen.
Position | a | b | c | d |
1 | 36.09 | 38.38 | 35.87 | 36.07 |
2 | 28.58 | 32.00 | 25.01 | 28.58 |
3 | 77.75 | 70.47 | 81.17 | 77.75 |
4 | 39.09 | 40.81 | 38.56 | 39.09 |
5 | 49.49 | 139.79 | 51.23 | 49.55 |
6 | 23.29 | 119.59 | 18.91 | 23.27 |
7 | 121.05 | 116.29 | 27.27 | 121.05 |
8 | 142.55 | 141.37 | 134.95 | 142.48 |
9 | 146.37 | 46.25 | 135.51 | 146.15 |
10 | 37.59 | 37.03 | 37.67 | 37.63 |
11 | 116.36 | 21.11 | 21.46 | 116.29 |
12 | 35.77 | 39.09 | 30.20 | 36.03 |
13 | 44.01 | 42.83 | 46.79 | 44.85 |
14 | 50.22 | 54.56 | 49.32 | 49.18 |
15 | 31.35 | 23.00 | 44.20 | 44.20 |
16 | 27.04 | 28.29 | 77.18 | 76.18 |
17 | 47.90 | 55.74 | 57.88 | 57.39 |
18 | 16.02 | 12.05 | 18.31 | 17.39 |
19 | 22.72 | 17.61 | 19.75 | 22.75 |
20 | 48.71 | 40.43 | 49.22 | 48.30 |
21 | 178.27 | 21.11 | 179.34 | 178.47 |
22 | 33.03 | 135.57 | 32.14 | 31.22 |
23 | 26.49 | 131.98 | 33.79 | 32.97 |
24 | 124.60 | 42.82 | 156.65 | 155.81 |
25 | 131.50 | 33.09 | 34.67 | 33.87 |
26 | 25.61 | 19.65 | 22.56 | 21.76 |
27 | 17.48 | 19.96 | 22.42 | 21.62 |
28 | 28.42 | 16.29 | 28.53 | 28.44 |
29 | 16.38 | - | 17.32 | 16.40 |
30 | 25.53 | - | 25.94 | 26.36 |
31 | - | - | 107.57 | 106.79 |
CH3CO | - | - | 21.68 | - |
CH3CO | - | - | 171.15 | - |